Mechanical
Construction | H-frame consisting of two vertical 65mm diameter chrome bars, base plate, crosshead and top plate. Area below barrel open Area above barrel guarded, access door with motor drive interlock |
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Frame strength | 290kN |
Stiffness | 100kN / mm drive to die (with 15mm bore) |
Safety | Interlocked guarding to protect operator from moving and high-temperature parts Crosshead force transducer to prevent mechanical damage Motor over-current trip Emergency stop switch Fume extraction 89/392/EEC & 91/368/EEC - machinery safety accreditation |
Barrel | Twin bore, 15mm diameter as standard (optional 20mm, 12mm) Bore length 280mm Three zone temperature control, RTD temperature sensors |
Dimensions | 2400mm(h) x 730mm(w) x 800mm(d) Weight 400kg |
Services | 220VAC (Single Phase) 50/60Hz 16A |
Drive
Type | 875W brushless motor driving recirculating ball screw |
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Feedback | 10,000 pulse encoder giving 0.02µm resolution |
Range | 0 to 50kN drive force 0.01mm/min to 500mm/min speed 50kN/500mm/min combination possible |
Drive modes | Constant speed 0.01mm/min to 500mm/min Constant pressure 1% full scale to 95% full scale Constant crosshead force 2kN to 45kN |
Temperature Control
Type | Three zone measurement and control |
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Sensors | Platinum resistance thermometers to DIN 43760 |
Control Range | Room temperature – 400°C (Standard) Room temperature – 500°C (Optional) |
Accuracy | ±0.5°C |
Uniformity | ±1.5°C throughout both barrel bores |
Instrumentation
Pressure transducers | One per bore, mounted just above the dies at equal heights |
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Ranges available | 3.45, 5.17, 6.9, 10.34, 20.69, 34.48, 51.72, 68.96, 103.45, 137.93, 206.9 MPa 10.34 and 68.96 MPa pressure transducers are included in the standard kit. |
Accuracy | ±0.25% full scale |
Temperature drift | 0.2psi/°C melt temperature |
Contact material | 15-5 PH with Amoloy coating |
Data conversion | 16-bit |
Force measurement | By transducer in crosshead. |
Melt temperature | By platinum resistance thermometer to DIN 43760 |
Flow rate | By 10,000ppr encoder on drive motor, resolution 0.02µm Accumulated position error <50µm full travel |
User channels | Five 4-20mA channels are available for connection to user-supplied measurement devices. The inputs are sampled at 16-bits, and the measurements may be recorded and manipulated within the RheoSolve software |
Dies
Type | Tungsten carbide |
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Tolerance | ±5µm diameter, ±10µm length |
Range | Length 0.25mm to 30mm Diameter 0.25mm to 5mm Entry angle 180° to 60° |
User Interface
Display | Backlit LCD display, showing machine operating status and barrel temperature |
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Input | Keypad and thumbwheel |
Functions | Crosshead up/down Set barrel temperature Diagnostics |
Software
The RheoSolve software is a single package that is used to configure experiments and to analyse the resulting data. It may also be used in stand-alone mode for offline analysis.
The software is designed for high productivity and includes many ease-of-use features and very powerful analysis and reporting. The user interface is highly configurable to let you work in the way you want, and a series of user levels can be defined to restrict access to certain features of the software so that less advanced users can use the software without the risk of producing invalid results.
Platform | Windows 2000/Vista/XP/7 |
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Recommended system | Pentium 4 2GHz, 128MB RAM, 40GB disk drive, 1280x1024 display resolution. A single USB port is required for connection to the rheometer. |
Rheometer control | Manual crosshead control Temperature zone control Pre-condition sample (thermal stabilisation and compression) Run pre-defined test Purge barrel contents |
Transducer database | Details of all transducer configuration, including calibration information, is held in a database, so working with multiple transducers is made more convenient. The software contains routines to assist with multi-point calibration of pressure and force transducers |
Die database | Database of available dies Support for capillary, orifice and rectangular slot dies |
Available test types | Shear rate sequence – twin bore Shear stress sequence (constant pressure) Thermal degradation tests Pressure vs volume test Melt fracture test Melt rupture test User defined test (script based) |
Data logging | Low-pass filtering available Recorded data: 2x pressure, 3x temperature, piston speed, piston position, time, user-defined acquisition channels |
Test information | Test progress bar Real time graphs of pressures, speed and position Real-time calculation and graphing of rheological properties |
Pressure equilibrium | Automatic or manual |
Basic analysis | Calculation of shear and extensional viscosity Calculation of power law index (n) Bagley and Rabinowitsch correction Non-Newtonian index Carreau, Cross, power law and log polynomial curve fits |
Derived curves | Shear rate, melt volume, volumetric flow rate |
User defined curves | Facility to use data from the standard channels (force, pressure, temperature), or user-provided measurement channels to derive further curves |
User defined analysis | A powerful set of functions is provided to allow user-defined calculations to be made on the captured data. |
Units | The software allows you to work in whatever units you choose – it provides by default SI, cgs and US units, but also allows you to define your own. All numeric quantities (measured data and documentation information) are recorded along with their units, and when results are calculated their resulting units are calculated too, ensuring consistency and greatly reducing the potential for errors. |
Documentation | Two types of documentation information are saved along with the test data: automatically recorded documentation (transducer and die information for example), and user-entered documentation. Documentation fields are configurable depending on your particular requirements, and fields can be made mandatory to ensure that critical information is recorded for every test. |
Graphs | Graphs are used for displaying measured and calculated data. Multiple tests and multiple quantities may be displayed on the same graph. Highly configurable appearance including colours, automatic or manual axis scaling, linear or logarithmic scaling, user-defined or automatic labelling. Graphs may be zoomed to examine the data in detail. |
Tables | Tables are used to display calculated results or documentation information. The results from multiple tests may be displayed in the same table. Flexible formatting includes colours, fonts, column headings, units and the format of numeric results. |
Data export | Data can be exported to Microsoft Excel (Office 95 onwards) in native file format. There is also the facility to export data in CSV (comma separated values) format, compatible with almost all numeric analysis packages. The software also includes a graphical editor to prepare curves for publishing. |
Test database | Test data may be saved either in individual files, or in a test database (Microsoft Access format). Multiple databases may be created, for different users or different applications. Test data stored in files may be copied into the database and vice versa. A powerful search tool can be used to interrogate the database and find tests that match particular criteria: for example, by the date of the test, the type of sample, a shear viscosity falling outside specified limits or a test performed at a particular temperature. |
Auto-save | An auto-save facility ensures that data from a test is never lost, and also imposes a consistent naming scheme for data files. Data can be automatically saved to files or to the test database. |
User levels | The software provides for three password-protected user levels. The software functions available to each level may be defined, preventing access to sensitive operations that might affect the accuracy of the data. |
Saving settings | Entire software configurations, or partial configurations, may be saved and later restored. This facility is useful both as a back-up mechanism and also to allow quick switching between different test types (for example, single bore and twin bore). |
Documentation | Full context sensitive help is available, together with a printed and an on-line manual. |
Options
Barrel |
Standard | Option |
Diameter | 15.0 mm | 12.0mm 20.0mm |
Material | Nitrided EN40C Steel (BS970 897M39) |
Hastelloy |
Length | 280 mm |
Drive |
Standard | Option |
Frame strength | 290kN |
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Max drive force | 50 kN (1) | 100 kN (1) |
Motor Power | 2,000 VA |
|
Max drive speed | 500 mm/min (1) | 1,000 mm/min (1) |
Speed Range | 50,000:1 (1) | 100,000:1(1) |
Speed Resolution | 1 part in 10,000 (1) | |
Notes | (1)Drive force is available and stable at all speeds (2)100kN and 1,000 mm/min options are not available together. |
Temperature Measurement |
Standard | Option |
Zones | 3 measurement zones + 3 control zones |
Added zones |
Temperature Ranges | 50 to 400 oC | 50 to 500 oC |
Other ranges are available as special orders | ||
Sensors | 3 units, Platinum Resistance Thermometers, type Pt-100 Accuracy better than 10 times DIN 43760 standard |
Temperature Control System |
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Control | Advanced algorithms using ( PID + DAC ) control loops |